Preconcentration of nickel and cobalt prior to their determination by graphite furnace atomic absorption spectrometry using the water-soluble polymer poly(vinyl pyrrolidinone)
Küçük Resim Yok
Tarih
2004
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Springer Wien
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
The use of a water-soluble polymer, poly(vinyl pyrrolidinone) (PVP), for the preconcentration and separation of nickel and cobalt prior to their determination by graphite furnace atomic absorption spectrometry is described. For this purpose, the sample and the water-soluble polymer solutions were mixed, and the metal-bound polymer was precipitated by pouring the mixture into acetone. The precipitate was separated by decantation and dissolved with distilled-deionized water. The analyte elements were determined by graphite furnace atomic absorption spectrometry. The validity of the method was tested with spiked sea water and mineral water samples. The analytes added to the samples were quantitatively recovered within the range of 95% confidence limits. The proposed technique is fast, simple, precise and inexpensive. Its low blank values and high precision are other important advantages.
Açıklama
Anahtar Kelimeler
Water-Soluble Polymer, Separation And Preconcentration, Trace Elements, Graphite Furnace Atomic Absorption Spectrometry, Trace Heavy-Metals, Mediated Extraction, Coprecipitation, Copper, Lead, Samples, Separation/Preconcentration, Sediment, Ions
Kaynak
Microchimica Acta
WoS Q Değeri
Q3
Scopus Q Değeri
Q1
Cilt
146
Sayı
1
