Monitoring of Pd in airborne particulates by solid sampling high-resolution continuum source electrothermal atomic absorption spectrometry

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dc.authoridBakircioglu Kurtulus, Yasemin/0000-0003-3013-5793
dc.authoridAkman, Suleyman/0000-0002-8625-783X
dc.authoridSzigeti, Tamas/0000-0001-5078-9503
dc.authorwosidBakircioglu Kurtulus, Yasemin/Q-2570-2017
dc.authorwosidBAYSAL, ASLI/L-6457-2014
dc.authorwosidAkman, Suleyman/C-1418-2014
dc.contributor.authorAtilgan, Semin
dc.contributor.authorAkman, Suleyman
dc.contributor.authorBaysal, Asli
dc.contributor.authorBakircioglu, Yasemin
dc.contributor.authorSzigeti, Tamas
dc.contributor.authorOvari, Mihaly
dc.contributor.authorZaray, Gyula
dc.date.accessioned2024-06-12T11:15:24Z
dc.date.available2024-06-12T11:15:24Z
dc.date.issued2012
dc.departmentTrakya Üniversitesien_US
dc.description.abstractAn analytical method has been developed for determination of palladium in PM2.5 fractions of urban airborne particulate matter by solid sampling high-resolution continuum source electrothermal atomic absorption spectrometry. For the optimization of the experimental conditions, a road dust certified reference material (BCR-723) was used. The influence of pyrolysis and atomization temperatures, the amount of sample introduced into the graphite furnace and the addition of acids, surfactants and modifiers on the analytical signal of Pd were investigated. The limit of detection, calculated based on three times the standard deviations of analytical signals obtained during the atomization of 10 blank filter pieces, was 0.07 pg/m(3). Since the amount of solid certified reference material introduced into the graphite furnace was about 50-2000 times lower than those required in order to obtain the certified value, the precision was relatively poor. This analytical method was applied for investigation of urban airborne particulate matter collected onto quartz fiber filters by high-volume aerosol samplers in the city center of Istanbul (Turkey) and Budapest (Hungary). The measured Pd concentrations changed in the range of 0.22-0.64 and 0.25-0.86 pg/m(3) in Istanbul and Budapest, respectively. (C) 2012 Elsevier B.V. All rights reserved.en_US
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [108Y328]; National Innovation Office of Hungary [OMFB-00582/2009]en_US
dc.description.sponsorshipThis study was supported by the Scientific and Technological Research Council of Turkey (TUBITAK project number: 108Y328) and the National Innovation Office of Hungary (Project number: OMFB-00582/2009) in framework of the Turkish-Hungarian collaboration agreement.en_US
dc.identifier.doi10.1016/j.sab.2012.04.008
dc.identifier.endpage38en_US
dc.identifier.issn0584-8547
dc.identifier.scopus2-s2.0-84862198071en_US
dc.identifier.scopusqualityQ2en_US
dc.identifier.startpage33en_US
dc.identifier.urihttps://doi.org/10.1016/j.sab.2012.04.008
dc.identifier.urihttps://hdl.handle.net/20.500.14551/23918
dc.identifier.volume70en_US
dc.identifier.wosWOS:000306044700004en_US
dc.identifier.wosqualityQ1en_US
dc.indekslendigikaynakWeb of Scienceen_US
dc.indekslendigikaynakScopusen_US
dc.language.isoenen_US
dc.publisherPergamon-Elsevier Science Ltden_US
dc.relation.ispartofSpectrochimica Acta Part B-Atomic Spectroscopyen_US
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanıen_US
dc.rightsinfo:eu-repo/semantics/closedAccessen_US
dc.subjectSolid Samplingen_US
dc.subjectHigh-Resolution Continuum Source Electrothermal Atomic Absorption Spectrometryen_US
dc.subjectPalladiumen_US
dc.subjectPM2.5en_US
dc.subjectPlatinum-Group Elementsen_US
dc.subjectRoad Dusten_US
dc.subjectUrban Areaen_US
dc.subjectPalladiumen_US
dc.subjectRhen_US
dc.subjectMatteren_US
dc.subjectRisken_US
dc.subjectParticlesen_US
dc.subjectCatalystsen_US
dc.subjectMetalsen_US
dc.titleMonitoring of Pd in airborne particulates by solid sampling high-resolution continuum source electrothermal atomic absorption spectrometryen_US
dc.typeArticleen_US

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