Determination of cadmium, copper, and zinc by flame atomic absorption spectrometry after preconcentration using a DETA (diethylenetriamine) polymer

Küçük Resim Yok

Tarih

2001

Dergi Başlığı

Dergi ISSN

Cilt Başlığı

Yayıncı

Marcel Dekker Inc

Erişim Hakkı

info:eu-repo/semantics/closedAccess

Özet

An atomic absorption spectrometric method with a preconcentration and separation procedure using a DETA (diethlyenetriamine) polymer is proposed for the determination of Cd, Cu and Zn. The influence various experimental condition on retention and elution efficiencies of the analyte were investigated by applying batch and column techniques. All investigated elements were quantitatively retained at pH 3, then were completely recovered by means of nitric acid. The loading capacity of the DETA polymer is 5.2 mg Cu2+/g polymer. A contact time of one minutes is sufficient for quantitative retention and elution which is shorter than for many Other sorbents. In the presence of sodium chloride up to 0.5% the analyte elements were quantitatively Separated and recovered.

Açıklama

Anahtar Kelimeler

Preconcentration, Cu, Cd, Zn, FAAS Diethylenetriamine, Silica-Gel, Activated Carbon, Water Samples, Separation, Metal, Collector, Elements, Resin, Lead

Kaynak

Analytical Letters

WoS Q Değeri

Q3

Scopus Q Değeri

Q3

Cilt

34

Sayı

3

Künye