Determination of cadmium, copper, and zinc by flame atomic absorption spectrometry after preconcentration using a DETA (diethylenetriamine) polymer
Küçük Resim Yok
Tarih
2001
Yazarlar
Dergi Başlığı
Dergi ISSN
Cilt Başlığı
Yayıncı
Marcel Dekker Inc
Erişim Hakkı
info:eu-repo/semantics/closedAccess
Özet
An atomic absorption spectrometric method with a preconcentration and separation procedure using a DETA (diethlyenetriamine) polymer is proposed for the determination of Cd, Cu and Zn. The influence various experimental condition on retention and elution efficiencies of the analyte were investigated by applying batch and column techniques. All investigated elements were quantitatively retained at pH 3, then were completely recovered by means of nitric acid. The loading capacity of the DETA polymer is 5.2 mg Cu2+/g polymer. A contact time of one minutes is sufficient for quantitative retention and elution which is shorter than for many Other sorbents. In the presence of sodium chloride up to 0.5% the analyte elements were quantitatively Separated and recovered.
Açıklama
Anahtar Kelimeler
Preconcentration, Cu, Cd, Zn, FAAS Diethylenetriamine, Silica-Gel, Activated Carbon, Water Samples, Separation, Metal, Collector, Elements, Resin, Lead
Kaynak
Analytical Letters
WoS Q Değeri
Q3
Scopus Q Değeri
Q3
Cilt
34
Sayı
3